Quantification of acrylamide in foods by Orbitrap high resolution mass spectrometry

Xianghui Kong; Antonio Dario Troise; Alberto Fiore; Vincenzo Fogliano

Quantification of acrylamide in foods by Orbitrap high resolution mass spectrometry

Xianghui Kong, Antonio Dario Troise, Alberto Fiore, Vincenzo Fogliano^*

^*Corresponding author for this work

Research output: Contribution to conference › Poster › peer-review

Abstract

Acrylamide detection still represents a hot topic in food chemistry. Solid phase clean up, liquid chromatography and tandem mass spectrometry are the golden standard procedure for its quantification. A method for acrylamide determination using high resolution mass spectrometry (HRMS) detection was developed. The procedure applied a simplified extraction and a 4 min chromatography. The mass accuracy was 0.1 ppm, the LOD 2.5 ng/mL and LOQ 5 ng/mL. The method was tested on cookies, French fries, ground coffee and brewed coffee. Results were in line with those obtained by tandem mass spectrometry.

Original language	English
Pages	156-158
Number of pages	3
Publication status	Published - Oct 2013
Externally published	Yes
Event	3rd MS Food Day - University of Trento, Trento, Italy Duration: 9 Oct 2013 → 11 Oct 2013 Conference number: 3rd https://www.fmach.it/CRI/info-generali/comunicazione/eventi-CRI/3rd-MS-Food-Day

Conference

Conference	3rd MS Food Day
Country	Italy
City	Trento
Period	9/10/13 → 11/10/13
Internet address	https://www.fmach.it/CRI/info-generali/comunicazione/eventi-CRI/3rd-MS-Food-Day

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Cite this

@conference{26a316f22f174a7db8cc516ca5235401,

title = "Quantification of acrylamide in foods by Orbitrap high resolution mass spectrometry",

abstract = "Acrylamide detection still represents a hot topic in food chemistry. Solid phase clean up, liquid chromatography and tandem mass spectrometry are the golden standard procedure for its quantification. A method for acrylamide determination using high resolution mass spectrometry (HRMS) detection was developed. The procedure applied a simplified extraction and a 4 min chromatography. The mass accuracy was 0.1 ppm, the LOD 2.5 ng/mL and LOQ 5 ng/mL. The method was tested on cookies, French fries, ground coffee and brewed coffee. Results were in line with those obtained by tandem mass spectrometry.",

author = "Xianghui Kong and Troise, {Antonio Dario} and Alberto Fiore and Vincenzo Fogliano",

year = "2013",

month = oct,

language = "English",

pages = "156--158",

note = "3rd MS Food Day ; Conference date: 09-10-2013 Through 11-10-2013",

url = "https://www.fmach.it/CRI/info-generali/comunicazione/eventi-CRI/3rd-MS-Food-Day",

}

TY - CONF

T1 - Quantification of acrylamide in foods by Orbitrap high resolution mass spectrometry

AU - Kong, Xianghui

AU - Troise, Antonio Dario

AU - Fiore, Alberto

AU - Fogliano, Vincenzo

N1 - Conference code: 3rd

PY - 2013/10

Y1 - 2013/10

N2 - Acrylamide detection still represents a hot topic in food chemistry. Solid phase clean up, liquid chromatography and tandem mass spectrometry are the golden standard procedure for its quantification. A method for acrylamide determination using high resolution mass spectrometry (HRMS) detection was developed. The procedure applied a simplified extraction and a 4 min chromatography. The mass accuracy was 0.1 ppm, the LOD 2.5 ng/mL and LOQ 5 ng/mL. The method was tested on cookies, French fries, ground coffee and brewed coffee. Results were in line with those obtained by tandem mass spectrometry.

AB - Acrylamide detection still represents a hot topic in food chemistry. Solid phase clean up, liquid chromatography and tandem mass spectrometry are the golden standard procedure for its quantification. A method for acrylamide determination using high resolution mass spectrometry (HRMS) detection was developed. The procedure applied a simplified extraction and a 4 min chromatography. The mass accuracy was 0.1 ppm, the LOD 2.5 ng/mL and LOQ 5 ng/mL. The method was tested on cookies, French fries, ground coffee and brewed coffee. Results were in line with those obtained by tandem mass spectrometry.

M3 - Poster

SP - 156

EP - 158

T2 - 3rd MS Food Day

Y2 - 9 October 2013 through 11 October 2013

ER -